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(1984) purge-and-trap GC/FID 0.1 µg/litre 99% Warner & Beasley (0.1 ppb) (1984) headspace/cryogenic trapping HR capillary 80 ng/litre 75% Comba & Kaiser GC/ECD (1983) Water and purge-and-trap GC 30 ng/litre 1.04-1.06C US EPA (1982b) wastewater 97.8% (method 601) grab sample GC/MS 4.7 µg/litre 1.02 + 0.45C US EPA (1982b) 99% (method 624) modified purge-and-trap GD/HECD and FID FID 0.1 µg/litre